Synthesis of carbon nanotubes and iron oxide nanoparticles in MW plasma torch with Fe(CO)5 in gas feed
Authors | |
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Year of publication | 2009 |
Type | Article in Periodical |
Magazine / Source | Applied Surface Science |
MU Faculty or unit | |
Citation | |
Field | Plasma physics |
Keywords | Carbon nanotube; Magnetite; Hematite; Iron pentacarbonyl |
Description | The MW plasma torch (2.45 GHz) in the mixture of CH4/H2/Ar (42/430/1540 sccm) with added Fe(CO)5vapors was used for the synthesis of iron oxide nanoparticles and carbon nanotubes. The particles with well/defined facets consisting of Fe3O4 and g-Fe2O3 and self-assembled into long chains were produced at the power of 360 W. At higher power of 440-460W the deposit contained significant amount of multi-walled carbon nanotubes covered by iron oxide nanoparticles. The diameter of CNTs was 8-20 nm. The particles had Fe3O4 and/or a-Fe2O3 cores of spherical shape covered by a thin layer of carbon. |
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